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Chemistry 2312
Instructor: Thomas R. Hoye
Fall 2020
Honors Organic Chemistry Laboratory (5 cr)
All files are PDFs (active links are blue; files to be added later are white)
SYLLABUS Chem 2312, Fall 2021
HANDOUTS
Synopsis of Experiments #1-5 and Lab Report Due Dates (posted on 9-6-21]
Lab Check-in Times and Round One (Week #1) Tutorial Schedules (posted 9-6-21)
Lab-open hours for Fall 2021 (posted on 9-7-21]
Hazardous (and non-Hazardous) Waste Handling Guidelines (posted 9-7-21)
Lab Report Guidelines
Properties of Common Organic Solvents, ranked by polarity (posted 9-11-21)
NMR Data Retrieval and MNova Installation Instructions (posted 9-14-21)
Instructions for installing Citrix Receiver (via Apps To Go) for accessing IRTutor, ChemDraw, and Chem 3D applications (posted 9-14-21)
Links to Technique Videos (posted 9-14-21)
Link to "Video: Mini-lab tour for undergraduate organic labs" at the Departmental NMR lab website (posted 9-14-21)
Video prepared by Alex Guzman showing how to 1) Download NMR data from the NMR lab server and 2) Install MNova (posted 9-16-21)
NMR Spectroscopy Tutorial (website from the Khan Academy; posted 9-16-21)
Infrared Spectroscopy Theory (PDF from U Colorado; posted 9-18-21)
Round Two (Weeks 3/4) Tutorial Schedule master (posted 09-28-21)
Vacuum Distillation Instructions (posted 09-28-21)
Spectroscopies Worksheet #1 (posted 9-30-21)
Epoxyphenoxypropane-161014 NMR Zipped Folder (posted 9-26-20)
Benzyl glycidyl ether-161014 NMR Zipped Folder (posted 9-26-20)
Notes on Computing Menthone Equilibrium Values (posted Oct 4, 2021)
Template (2 page PDF) for Creating Your Excel Spreadsheet for the Menthone Boltzmann Equilibrium Values (posted Oct 4, 2021)
Instructions for Accessing Maestro at MSI via Nice (a Linux desktop emulator) (posted 10-6-21)
Coll Czech Chem Comm '89 151-159 (posted 10-7-21)
Zip file of the 1H NMR spectrum of a bromofluorotoluene (of a different substitution pattern of your X or Y) (posted 10-7-21)
Zip file of the 13C NMR spectrum of the same bromofluorotoluene (of a different substitution pattern of your X or Y) (posted 10-7-21)
MNova file of the 1H NMR spectrum of "X" in C6D6 (posted 10-7-21)
MNova file of the 1H NMR spectrum of "Y" in DMSO-d6 (posted 10-7-21)
Coupling Constant Analysis; J. Org. Chem. 2002, 67, 4014–4016 (posted 10-20-21)
Spectroscopies Worksheet #2 (posted 11-8-21)
MNova file of isomenthone 1D and 2D spectra (posted 11-8-21)
Slide clip from Mosher Ester discussed in class 10-22-20 (posted 10-22-20)
Schedule of Times for your Access to the Ozone Generator (posted 09-25-20) Not needed in F'21
X-ray structure .pdb file of the atomic co-ordinates of the amide structure (posted 11-14-21): see UPDATED Experiment #3 for instructions on how to view (via iCn3D, on a browser)
EXPERIMENTS
Exp 1. Ketone Reduction (posted 9-8-21)
Exp 2. Ozonolysis (of beta-Pinene) and Hydrogenation (of Pulegone) (posted 9-22-21)
Exp 3. Ester Enolate Alkylation/Saponification/DCC Amide Coupling (UPDATE posted 11-14-21)
Exp 4. Palladium Coupling, Lipase Kinetic Resolution, Mosher Ester Analysis (posted 10-7-21)
Exp 5. Diels-Alder Reaction, Luche Reduction, and Photochemical 2+2 Cycloaddition (posted 10-12-21)
Staggerred Schedule for Experiments 3-5 (posted 10-7-21)
ZOOM RECORDINGS
Zoom Recording from ad hoc lecture on Saturday 9-11-21
Zoom Recording (1 of 2) from ad hoc lecture on Saturday 9-18-21
Zoom Recording (2 of 2) from ad hoc lecture on Saturday 9-18-21
iPAD NOTES TO ACCOMPANY ANY ZOOM RECORDINGS
iPad Notes from ad hoc lecture on 9-11-21
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